卷烟搭口胶的裂解气相色谱-质谱分析

卷烟搭口胶是用在卷烟制造过程中必不可少的辅助材料,由于它直接参与烟支燃烧,因此对卷烟的产品质量和生物安全具有较大的影响.     

能动抛光磨盘的变形实验研究

 能动抛光磨盘实时产生不同的表面变形，在对大口径非球面光学元件进行精磨和抛光时实现与工件表面良好的大尺寸吻合，可以消除传统光学加工采用小尺寸磨头时带来的高频残余误差并提高加工效率。以加工直径1.3m左右，F/2的抛物面光学元件为例，对能动磨盘在不同离轴度时能够产生的变形进行了计算和实验。结果表明，能动磨盘能够以较高精度产生旋转对称或非对称的抛物面形状。对能动磨盘产生变形后的残余误差进行了分析。     

An Investigation into the Migration of Segments in Crosslinked Fluorinated Polyimide Adhesive

Crosslinked fluorinated polyimides (CFPI) were successfully synthesized to study and explore the effect of cross-linkage on the migration of fluorinated segments and on the adhesion strength. Characterization by dynamic thermomechanical analysis (DMA) and thermo gravimetric analysis (TGA) confirmed good thermal properties of CFPI. X-ray photoelectron spectroscopy (XPS) results showed that the ratio of fluorinated component (6FDA-ODA) concentration of the surface to the bulk decreased with the crosslink density. The water contact angle of CFPI was lower than that of non-crosslinked fluorinated polyimide, indicating that the migration of fluorinated groups to the surface was reduced by the presence of cross-linkage. Therefore, CFPI, with no fluorine segregation on the surface, exhibited excellent wetting of adherent surfaces and adhesion strength, which was proved by lap shear strength (LSS) measurements and scanning electron microscopy.     

点支撑预应力中厚矩形板的弯曲

基于Reissner-Mindlin一阶剪切变形板理论，讨论在预加面内机械荷载或温度场作用下，点支撑中厚矩形板的弯曲问题。温度场假定沿板表面为均布，沿板厚方向为线性分布的。利用考虑剪切变形影响的Timoshenko梁函数，采用Rayleigh-Ritz法给出不同边界条件下点支撑中厚板在横向荷载作用下的挠度和弯矩分布。结果表明，均匀温度场与预加面内压力将使板的挠度和弯矩增加。支撑点位置的变化、边界约束条件和横向剪切变形效应都对板的内力大小和分布有显著影响。     

胶粘剂拉伸剪切强度测量结果的不确定度评定

依据GB/T 7124-2008《胶粘剂拉伸剪切强度的测定》,以环氧树脂结构胶为例,对胶粘剂拉伸剪切强度测量结果的不确定度分量进行了分析和量化,计算了合成标准不确定度和扩展不确定度。当环氧树脂结构胶的拉伸剪切强度为28.8 MPa时,扩展不确定度为1.0 MPa(k=2)。     

单轴〈111〉应力硅价带结构计算

基于k·p微扰法计算了单轴〈111〉应力作用下硅的价带结构, 并与未受应力时体硅的价带结构进行了比较. 给出了单轴〈111〉应力作用下硅价带顶处能级的移动、分裂以及空穴有效质量的变化情况. 计算所得未受应力作用时硅价带顶处重空穴带、轻空穴带有效质量与相关文献报道体硅有效质量结果一致. 拓展了单轴应力硅器件导电沟道应力与晶向的选择范围,给出的硅价带顶处重空穴带、轻空穴带能级间的分裂值和有效质量随应力的变化关系可为单轴〈111〉应力硅其他物理参数的计算提供参考. 关键词： 单轴应力硅 k·p法')" href="#">k·p法 价带结构     

能动抛光磨盘的有限元法分析

 能动磨盘在光学抛光时随磨盘移动位置和旋转角度不同而产生不同的变形以实时与大口径被抛光工件表面实现良好的吻合。模拟了能动磨盘的工作过程，探讨了用于光学抛光的可行性。以加工直径1.5m，f1/2的抛物面光学元件为例，用有限元法对能动磨盘能够产生的变形进行了仿真计算，结果表明能动磨盘能够以较高精度产生旋转对称或非对称的二次曲面。     

Dependency of dynamic interlaminar shear strength of composites on test technique used

Studies are presented on dependency of dynamic interlaminar shear (ILS) strength on the experimental technique used for a typical plain weave E-glass/epoxy composite. Dynamic ILS strength was determined based on two experimental techniques, namely torsional split Hopkinson bar (TSHB) apparatus using thin walled tubular specimens and compressive split Hopkinson pressure bar (SHPB) apparatus using single lap specimens. The results obtained from these techniques are compared. In general, it is observed that dynamic ILS strength for composites obtained by TSHB testing using thin walled tubular specimens is lower than the dynamic ILS strength obtained using single lap specimens in compressive SHPB. The issues involved in TSHB testing of thin walled tubular specimens made of composites are discussed and the reasons for reduced dynamic ILS strength using thin walled tubular specimens are highlighted. Finite element analysis (FEA) of thin walled tubular specimens made of composite and resin subjected to quasi-static torsional loading is presented. Using FEA results, the reasons for lower ILS strength of composite thin walled tubular specimens are substantiated.     

主动抛光盘面形测试技术的研究

主动抛光盘技术是新发展起来的一种能够根据需要将抛光盘面实时地主动变形成离轴非球面来磨制深非球度高精度天文镜面的磨制技术。简单介绍了抛光盘变形控制结构和面形检测机构，对深非球面度面形变形进行了精度分析，探讨了主动抛光盘的动态响应和校正，并对抛光盘的改造提出了一些建议。     

能动磨盘变形检测中的各误差因素分析

针对现有f530 mm能动磨盘的检测系统（有效检测口径f420 mm）,系统分析了检测过程中的球头误差、传感器安装角度误差和坐标定位误差,并给出了各项误差对检测精度的影响。同时,还针对检测基座不完全水平的问题建立模型,应用最小二乘法实现了检测数据的去倾斜处理。给出了实测数据去倾斜前后和误差补偿前后的检测精度对比情况,结果表明去倾斜算法能较好地还原实测数据,补偿检测中的系统误差有助于提高检测精度。